Tetrasulfide Silane Coupling Agent Crosile® 69 for Rubber

Silane coupling agent Crosile®69 is bifunctional, sulfur-containing organosilane for rubber applications in combination with white fillers containing silanol groups

Chemical Name
Bis [3-(triethoxysilyl)propyl] tetrasulfide
CAS NO.  
40372-72-3
Formula
(C2H5O)3SiCH2CH2CH2-S4-CH2CH2CH2Si(OC2H5)3
Formula Structure

 

Chemical Properties

Silane coupling agent Crosile® 69 Bis[3-(triethoxysilyl)propyl]tetrasulfide (TESPTS) is commonly used as a crosslinking agent and reinforcing filler in rubber manufacturing. TESPT Crosile®69 films provide corrosion protection to metal substrates. It is also used as a precursor for the synthesis of mesoporous silicones.

 

Equivalent Type

Bis(3-triethoxysilylpropyl)tetrasulfane, Bis(3-(ethoxysilyl)propyl)tetrasulfide, Bis(triethoxysilylpropyl)tetrasulfane, Bis[3-(triethoxysilyl)propyl]tetrasulfide, Tetrasulfane, Bis(3-Triethoxysilylpropyl)-, Silane coupling agent,

 

Specifications

Properties Units Target Values

(Spec,Limits)

Alcohol content %(wt) ≤0.5%
CLPTES Content %(wt) ≤3.0%
Other impurity content %(wt) ≤1.0%
Viscosity 25°C (cps) Cps ≤14.0
Sulfur Content %(wt) 22.5(21.7-23.3)
Average chain Length 3.70(3.55-3.85)
S2 content % ( wt) 18.0(15.0-21.0)
S3 content % (wt) 30.0(27.0-33.0)
S4 content % (wt) 24.0(21.0-27.0)
S5 to S8 content % ( wt) 27.0(24.0-30.0)
Volatility (100°C /10min.) % ≤ 1.0%
Specific Gravity (25°C) 1.080 ± 0.020
Refractive Index (25°C) 1.480 ± 0.020

 

Application

1. Crosile® 69 is a kind of multifunctional silane coupling agent that has been used successfully in the rubber industry. It is used to improve physical and mechanical properties of vulcanizates.
2. Crosile® 69is able to markedly improve tensile strength, tearing strength and abrasive resistance and reduce compression set of vulcanizates. In addition, it can reduce the viscosity and improve the processability of rubber products.
3. Crosile® 69 is especially suitable to improve the reinforcing properties of fillers that contain hydroxyl groups in all unsaturated polymers having double bonds or their blends. Silica, talc powder, mica powder and clay can be used in combination with crosile-69 in polymers such as NR, IR, SBR, BR, NBR and EPDM.
Recommend dosage 1.0-4.0 PHR

Bis[γ-(triethoxysilyl)propyl]tetrasulfide,Bis-[γ-(triethoxysilyl)-propyl]-tetrasulfide,Silane Coupling Agent Si-69,Silane Coupling Agent A-1289,Silane Coupling Agent KH-858,Bis-[3-(triethoxysilylpropyl)]-tetrasulfide

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